Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid

Base Information

Chemical Name:Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid
CAS No.:106948-00-9
Molecular Formula:C₁₇H₂₁NO₇
Molecular Weight:351.356
Hs Code.:

Synonyms:Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid

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Chemical Property of Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid

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Technology Process of Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid

There total 6 articles about Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 106947-99-3
Methyl-2-benzamido-6-O-benzoyl-2-desoxy-5-O-mesyl-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucofuranosid

: 106948-00-9
Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid

Guidance literature:: With sodium methylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

Reference yield:

: 106947-89-1
Methyl-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-β-D-glucofuranosid

: 106948-00-9
Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 58 percent / DCC, DMAP / tetrahydrofuran / 24 h / Ambient temperature

2: 58 percent / pyridine / 16 h / -10 °C

3: 54 percent / pyridine / 16 h / Ambient temperature

4: 93 percent / CH₃ONa / tetrahydrofuran / 0.5 h / 0 °C

With pyridine; dmap; sodium methylate; dicyclohexyl-carbodiimide; In tetrahydrofuran;

Reference yield:

: 3804-93-1
(R)-2-[(3aR,5S,6R,6aR)-5-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazol-6-yloxy]-propionic acid

: 106948-00-9
Methyl-5,6-anhydro-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-α-L-idofuranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / 168 h / Ambient temperature

2: 86 percent / 60percent aq. CH₃COOH / 23 h / Ambient temperature

3: 58 percent / DCC, DMAP / tetrahydrofuran / 24 h / Ambient temperature

4: 58 percent / pyridine / 16 h / -10 °C

5: 54 percent / pyridine / 16 h / Ambient temperature

6: 93 percent / CH₃ONa / tetrahydrofuran / 0.5 h / 0 °C

With pyridine; dmap; sodium methylate; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran;