[1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine

Base Information

Chemical Name:[1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine
CAS No.:181868-73-5
Molecular Formula:C₂₀H₂₁BrN₂O₂S
Molecular Weight:433.369
Hs Code.:

Synonyms:[1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine

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Chemical Property of [1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine

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Technology Process of [1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine

There total 2 articles about [1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 136878-59-6
[1-(1-Benzenesulfonyl-2-methyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine

: 181868-73-5
[1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine

Guidance literature:: With N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; for 1.5h; Heating;
DOI:10.1021/jo9607929

Reference yield:

: 124293-81-8
1-(benzenesulfonyl)-2-methyl-1H-indole-3-carbaldehyde

: 181868-73-5
[1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 4 Angstroem molecular sieves / CH₂Cl₂ / 4 h / Heating

2: 89 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 1.5 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; 4 A molecular sieve; In tetrachloromethane; dichloromethane;
DOI:10.1021/jo9607929

Reference yield:

: 181868-73-5
[1-(1-Benzenesulfonyl-2-bromomethyl-1H-indol-3-yl)-meth-(E)-ylidene]-tert-butyl-amine

: 181868-75-7
1-Benzenesulfonyl-2-ethanesulfinylmethyl-1H-indole-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) DBU, 2.) 2N HCl / 1.) benzene, room temperature, 2 h, 2.) acetone, room temperature, 30 min

2: 92 percent / aq. NaIO₄ / dioxane / Ambient temperature

With hydrogenchloride; sodium periodate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane;
DOI:10.1021/jo9607929