Technology Process of (E)-9-benzoyloxy octadec-10-en-12-yn-1-al
There total 10 articles about (E)-9-benzoyloxy octadec-10-en-12-yn-1-al which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) Mg / 1.) THF/ether, reflux, 4 h; 2.) THF/ether, 6 h, r.t.
2: 83 percent / pyridine / Ambient temperature
3: 75 percent / PPTS / ethanol / 2 h / 55 °C
4: 71 percent / pyridinium dichromate / CH2Cl2 / 6 h / Ambient temperature
With
pyridine; dipyridinium dichromate; pyridinium p-toluenesulfonate; magnesium;
In
ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)87295-1
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 70 percent / 48percent HBr / toluene / 6 h / Heating
2: 90 percent / p-TsOH / CH2Cl2 / 3 h / Ambient temperature
3: 1.) Mg / 1.) THF/ether, reflux, 4 h; 2.) THF/ether, 6 h, r.t.
4: 83 percent / pyridine / Ambient temperature
5: 75 percent / PPTS / ethanol / 2 h / 55 °C
6: 71 percent / pyridinium dichromate / CH2Cl2 / 6 h / Ambient temperature
With
pyridine; dipyridinium dichromate; hydrogen bromide; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; magnesium;
In
ethanol; dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)87295-1
