cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate

Base Information

Chemical Name:cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate
CAS No.:1192836-57-9
Molecular Formula:C₂₁H₂₆N₄O₄S
Molecular Weight:430.528
Hs Code.:

Synonyms:cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate

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Chemical Property of cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate

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Technology Process of cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate

There total 3 articles about cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 354812-10-5
2-[(aminocarbonyl)amino]-5-bromo-3-thiophenecarboxamide

: 1192836-40-0
cyclopentyl N-[3-(dihydroxyboryl)benzyl]-L-alaninate

: 1192836-57-9
cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate

Guidance literature:: With potassium acetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; at 90 ℃; Sealed vial;

Reference yield:

: 96-41-3
Cyclopentanol

: 1192836-57-9
cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hexane / 12 h / 135 °C

2.1: sodium tris(acetoxy)borohydride / dichloromethane / 2.33 h / 20 °C

2.3: pH 7

3.1: potassium acetate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 90 °C / Sealed vial

With potassium acetate; sodium tris(acetoxy)borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; hexane; dichloromethane; toluene;

Reference yield:

: 261909-89-1
(S)-cyclopentyl 2-aminopropanoate 4-methylbenzenesulphonic acid

: 1192836-57-9
cyclopentyl N-{3-[4-carbamoyl-5-(carbamoylamino)-2-thienyl]benzyl}-L-alaninate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tris(acetoxy)borohydride / dichloromethane / 2.33 h / 20 °C

1.3: pH 7

2.1: potassium acetate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 90 °C / Sealed vial

With potassium acetate; sodium tris(acetoxy)borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; toluene;