trimethyl 4,4′,4′′-[{[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(azanediyl)}tris(carbonyl)]tribenzoate

Base Information

Chemical Name:trimethyl 4,4′,4′′-[{[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(azanediyl)}tris(carbonyl)]tribenzoate
CAS No.:1523492-70-7
Molecular Formula:C₃₉H₃₉N₃O₁₂
Molecular Weight:741.752
Hs Code.:

Synonyms:trimethyl 4,4′,4′′-[{[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(azanediyl)}tris(carbonyl)]tribenzoate

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Chemical Property of trimethyl 4,4′,4′′-[{[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(azanediyl)}tris(carbonyl)]tribenzoate

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Technology Process of trimethyl 4,4′,4′′-[{[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(azanediyl)}tris(carbonyl)]tribenzoate

There total 2 articles about trimethyl 4,4′,4′′-[{[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(azanediyl)}tris(carbonyl)]tribenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1679-64-7
Monomethyl terephthalate

: (2,4,6-trimethoxybenzene-1,3,5-triyl)trimethanamine hydrobromide

: 1523492-70-7
trimethyl 4,4′,4′′-[{[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(azanediyl)}tris(carbonyl)]tribenzoate

Guidance literature:: Monomethyl terephthalate; With iodine; triethylamine; phosphorous acid trimethyl ester; In dichloromethane; for 0.333333h; Cooling;

(2,4,6-trimethoxybenzene-1,3,5-triyl)trimethanamine hydrobromide; In dichloromethane; at 0 - 25 ℃; for 3.17h;
DOI:10.1055/s-0033-1339639

Reference yield:

: 434323-17-8
1,3,5-tris(bromomethyl)-2,4,6-(trimethoxy)benzene

: 1523492-70-7
trimethyl 4,4′,4′′-[{[(2,4,6-trimethoxybenzene-1,3,5-triyl)tris(methylene)]tris(azanediyl)}tris(carbonyl)]tribenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonia / 18 h / 25 °C / Sealed tube

2.1: phosphorous acid trimethyl ester; triethylamine; iodine / dichloromethane / 0.33 h / Cooling

2.2: 3.17 h / 0 - 25 °C

With ammonia; iodine; triethylamine; phosphorous acid trimethyl ester; In dichloromethane;
DOI:10.1055/s-0033-1339639