O'1,O₁-([1,1'-biphenyl]-4,4'-diylbis(2-oxoethane-2,1-diyl)) 1-diethyl bis(cyclobutane-1,1-dicarboxylate)

Base Information

• Chemical Name: O'1,O₁-([1,1'-biphenyl]-4,4'-diylbis(2-oxoethane-2,1-diyl)) 1-diethyl bis(cyclobutane-1,1-dicarboxylate)
• CAS No.: 1447941-04-9
• Molecular Formula: C₃₂H₃₄O₁₀
• Molecular Weight: 578.616
• Mol file: 1447941-04-9.mol

Synonyms:O'1,O₁-([1,1'-biphenyl]-4,4'-diylbis(2-oxoethane-2,1-diyl)) 1-diethyl bis(cyclobutane-1,1-dicarboxylate)

Chemical Property of O'1,O₁-([1,1'-biphenyl]-4,4'-diylbis(2-oxoethane-2,1-diyl)) 1-diethyl bis(cyclobutane-1,1-dicarboxylate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O'1,O₁-([1,1'-biphenyl]-4,4'-diylbis(2-oxoethane-2,1-diyl)) 1-diethyl bis(cyclobutane-1,1-dicarboxylate)

There total 1 articles about O'1,O₁-([1,1'-biphenyl]-4,4'-diylbis(2-oxoethane-2,1-diyl)) 1-diethyl bis(cyclobutane-1,1-dicarboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-bis(bromoacetyl)biphenyl (4072-67-7) + ethyl hydrogen cyclobutane-1,1-dicarboxylate (54450-84-9) → O'1,O1-([1,1'-biphenyl]-4,4'-diylbis(2-oxoethane-2,1-diyl)) 1-diethyl bis(cyclobutane-1,1-dicarboxylate) (1447941-04-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In chloroform; acetonitrile; at 20 ℃;

Reference yield:

O'1,O1-([1,1'-biphenyl]-4,4'-diylbis(2-oxoethane-2,1-diyl)) 1-diethyl bis(cyclobutane-1,1-dicarboxylate) (1447941-04-9) → diethyl 1,1'-(4,4'-(biphenyl-4,4'-diyl)bis(1H-imidazole-4,2-diyl))dicyclobutanecarboxylate (1447941-05-0)

Guidance literature:

With ammonium acetate; In 5,5-dimethyl-1,3-cyclohexadiene; at 135 ℃; for 3h; Sealed tube;

upstream raw materials:

4,4'-bis(bromoacetyl)biphenyl

ethyl hydrogen cyclobutane-1,1-dicarboxylate

Downstream raw materials:

diethyl 1,1'-(4,4'-(biphenyl-4,4'-diyl)bis(1H-imidazole-4,2-diyl))dicyclobutanecarboxylate