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1-methyl-3-(perfluoropropan-2-yl)benzene

Base Information
  • Chemical Name:1-methyl-3-(perfluoropropan-2-yl)benzene
  • CAS No.:51114-11-5
  • Molecular Formula:C10H7F7
  • Molecular Weight:260.154
  • Hs Code.:
1-methyl-3-(perfluoropropan-2-yl)benzene

Synonyms:1-methyl-3-(perfluoropropan-2-yl)benzene

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Chemical Property of 1-methyl-3-(perfluoropropan-2-yl)benzene
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Technology Process of 1-methyl-3-(perfluoropropan-2-yl)benzene

There total 3 articles about 1-methyl-3-(perfluoropropan-2-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
1-methyl-3-(perfluoroprop-1-en-2-yl)benzene; With 4-tolyl iodide; Olah′s reagent; In chloroform; at 20 ℃; for 0.0166667h;
With Selectfluor; In chloroform; at 50 ℃; for 24h; Sealed tube;
DOI:10.1055/a-1485-4916
Guidance literature:
Multi-step reaction with 2 steps
1.1: triphenylphosphine / N,N-dimethyl-formamide / 0.5 h / 105 °C
2.1: 4-tolyl iodide; Olah′s reagent / chloroform / 0.02 h / 20 °C
2.2: 24 h / 50 °C / Sealed tube
With 4-tolyl iodide; Olah′s reagent; triphenylphosphine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1055/a-1485-4916
Guidance literature:
m-Iod-toluol, Iodid 2 in Ggw. v. Cu in DMF bei 135-145grad;
upstream raw materials:

3'-methyl-2,2,2-trifluoroacetophenone

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