Technology Process of C29H37NO5
There total 7 articles about C29H37NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
In
dichloromethane;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1039/c2ob26649k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / diethyl ether / 2.25 h / 0 - 20 °C / Inert atmosphere
2: sodium azide / N,N-dimethyl-formamide / 20 h / Inert atmosphere; Heating
3: triphenylphosphine / tetrahydrofuran; water / 3 h / 70 °C / Inert atmosphere
4: dichloromethane / 6 h / Inert atmosphere; Irradiation
5: dmap; pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere
With
pyridine; dmap; sodium azide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
3: |Staudinger Azide Reduction;
DOI:10.1039/c2ob26649k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide / N,N-dimethyl-formamide / 20 h / Inert atmosphere; Heating
2: triphenylphosphine / tetrahydrofuran; water / 3 h / 70 °C / Inert atmosphere
3: dichloromethane / 6 h / Inert atmosphere; Irradiation
4: dmap; pyridine / dichloromethane / 12 h / 20 °C / Inert atmosphere
With
pyridine; dmap; sodium azide; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
2: |Staudinger Azide Reduction;
DOI:10.1039/c2ob26649k
