4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-ethynylphenyl)-20-porphinyl]diphenylethyne

Base Information

Chemical Name:4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-ethynylphenyl)-20-porphinyl]diphenylethyne
CAS No.:184154-23-2
Molecular Formula:C₁₀₉H₈₈N₈Zn₂
Molecular Weight:1640.73
Hs Code.:

Synonyms:4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-ethynylphenyl)-20-porphinyl]diphenylethyne

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Chemical Property of 4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-ethynylphenyl)-20-porphinyl]diphenylethyne

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Technology Process of 4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-ethynylphenyl)-20-porphinyl]diphenylethyne

There total 1 articles about 4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-ethynylphenyl)-20-porphinyl]diphenylethyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 184154-22-1
4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-[2-(trimethylsilyl)ethynyl]phenyl)-20-porphinyl]diphenylethyne

: 184154-23-2
4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-ethynylphenyl)-20-porphinyl]diphenylethyne

Guidance literature:: With tetrabutyl ammonium fluoride; In chloroform; stirring (room temp., 30 min); evapn. of the org. layer, chromy.;
DOI:10.1021/ja961611n

Reference yield: 80.0%

: 5-(4-iodophenyl)-10,15,20-tris(2,4,6-trimethylphenyl)porphyrin

: 184154-23-2
4-[zinc(II) 5,10,15-trimesityl-20-porphyrinyl]-4'-[zinc(II) 5,15-dimesityl-10-(2,6-dimethyl-4-ethynylphenyl)-20-porphinyl]diphenylethyne

: ZnC₂₀H₈N₄(C₆H₂(CH₃)3)3C₆H₄CCC₆H₄ZnC₂₀H₈N₄(C₆H₂(CH₃)3)2C₆H₂(CH₃)2CCC₆H₄C₂₀H₁₀N₄(C₆H₂(CH₃)3)3

Guidance literature:: In triethylamine; toluene; anaerobic conditions, 35°C (2 h), catalysator Pd2(dba)3 with AsPh3; chromatographic workup;
DOI:10.1021/ja961611n