4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene

Base Information

Chemical Name:4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene
CAS No.:1246962-64-0
Molecular Formula:C₂₇H₃₂N₆O₄
Molecular Weight:504.589
Hs Code.:

Synonyms:4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene

Suppliers and Price of 4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene

There total 12 articles about 4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 557-21-1
zinc(II) cyanide

: 1246962-62-8
4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dibromopyridin-4-ylazo)benzene

: 1246962-64-0
4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene

Guidance literature:: With copper(l) cyanide; In dimethyl sulfoxide; at 95 - 100 ℃; for 4h; Inert atmosphere;
DOI:10.1007/s10593-010-0528-8

Reference yield: 33.0%

: 557-21-1
zinc(II) cyanide

: 1246962-62-8
4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dibromopyridin-4-ylazo)benzene

: 1246962-63-9
4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3-bromo-5-cyanopyridin-4-ylazo)-benzene

: 1246962-64-0
4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene

Guidance literature:: With copper(l) cyanide; In N,N-dimethyl-formamide; at 90 ℃; for 1h; Inert atmosphere;
DOI:10.1007/s10593-010-0528-8

Reference yield:

: 84539-34-4
4-amino-3,5-dibromopyridine

: 1246962-64-0
4-[N,N-bis(2-tetrahydro-2H-pyran-2-yloxyethyl)amino]-1-(3,5-dicyanopyridin-4-ylazo)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid; phosphoric acid; isopentyl nitrite / 1 h / -10 - -5 °C

1.2: 1 h / 10 - 20 °C

2.1: N,N-dimethyl-formamide / 24 h / 40 - 45 °C

3.1: copper(l) cyanide / dimethyl sulfoxide / 4 h / 95 - 100 °C / Inert atmosphere

With phosphoric acid; nitric acid; copper(l) cyanide; isopentyl nitrite; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1007/s10593-010-0528-8