tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane

Base Information

Chemical Name:tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane
CAS No.:1266383-97-4
Molecular Formula:C₄₁H₇₄Cl₄O₄Si₂
Molecular Weight:829.019
Hs Code.:

tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane

Synonyms:tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane

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Chemical Property of tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane

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Technology Process of tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane

There total 18 articles about tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 1266383-82-7
(5S,6S,8R)-17,17-dichloro-5-[(1S,2R)-1,2-dichlorooctyl]-2,2,3,3,20,20,21,21-octamethyl-4,19-dioxa-3,20-disiladocosane-6,8-diol

: 1266383-97-4
tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃; for 2.83333h;
DOI:10.1021/ol1029518

Reference yield:

: 4,5-dichloroundec-1-en-3-ol

: 1266383-97-4
tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane

Guidance literature:: Multi-step reaction with 6 steps

1: vinyl acetate; lipase PS IM Amano; triethylamine / tert-butyl methyl ether / 120 h / 20 °C / Enzymatic reaction

2: 2,6-dimethylpyridine / dichloromethane / 0.83 h / 20 °C

3: phenyl isocyanate; triethylamine / toluene / 20 - 90 °C

4: water; molybdenum hexacarbonyl / acetonitrile / 20 - 90 °C

5: acetic acid; tetramethylammonium triacetoxyborohydride / dichloromethane; acetonitrile / 1 h / 20 °C

6: pyridinium p-toluenesulfonate / dichloromethane / 2.83 h / 20 °C

With 2,6-dimethylpyridine; vinyl acetate; lipase PS IM Amano; water; pyridinium p-toluenesulfonate; phenyl isocyanate; acetic acid; triethylamine; tetramethylammonium triacetoxyborohydride; molybdenum hexacarbonyl; In dichloromethane; tert-butyl methyl ether; toluene; acetonitrile;
DOI:10.1021/ol1029518

Reference yield:

: 1159428-45-1
1-(tert-butyldimethylsilyloxy)-2,2-dichloro-11-iodoundecane

: 1266383-97-4
tert-butyl(10-{(2R,4R,6S)-6-[(1S,2S,3R)-1-(tert-butyldimethylsiloxy)-2,3-dichlorononyl]-2-phenyl-1,3-dioxan-4-yl}-2,2-dichlorodecyloxy)dimethylsilane

Guidance literature:: Multi-step reaction with 5 steps

1: sodium nitrite / N,N-dimethyl-formamide / 0.33 h / 20 °C

2: phenyl isocyanate; triethylamine / toluene / 20 - 90 °C

3: water; molybdenum hexacarbonyl / acetonitrile / 20 - 90 °C

4: acetic acid; tetramethylammonium triacetoxyborohydride / dichloromethane; acetonitrile / 1 h / 20 °C

5: pyridinium p-toluenesulfonate / dichloromethane / 2.83 h / 20 °C

With water; pyridinium p-toluenesulfonate; phenyl isocyanate; acetic acid; triethylamine; tetramethylammonium triacetoxyborohydride; sodium nitrite; molybdenum hexacarbonyl; In dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol1029518