2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione

Base Information

Chemical Name:2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione
CAS No.:1544673-61-1
Molecular Formula:C₂₂H₂₄BNO₄
Molecular Weight:377.248
Hs Code.:

Synonyms:2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione

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Chemical Property of 2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione

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Technology Process of 2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione

There total 5 articles about 2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₃BO₅S

: 1074-82-4
potassium phtalimide

: 1544673-61-1
2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.3390/molecules181012346

Reference yield:

: 1106869-99-1
(3-formyl-4-methylphenyl)boronic acid

: 1544673-61-1
2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: magnesium sulfate / methanol / 6 h / 20 °C

2: sodium tetrahydroborate / 5 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/molecules181012346

Reference yield:

: 1352132-34-3
2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde

: 1544673-61-1
2-[2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / 5 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C

With sodium tetrahydroborate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/molecules181012346