2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline

Base Information

Chemical Name:2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline
CAS No.:79365-94-9
Molecular Formula:C₄₆H₄₄N₂O₁₅
Molecular Weight:864.86
Hs Code.:

Synonyms:2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline

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Chemical Property of 2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline

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Technology Process of 2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline

There total 5 articles about 2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50604-74-5
2-acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3-O-acetyl-1,6-anhydro-2-deoxy-β-D-glucopyranose

: 79365-94-9
2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline

Guidance literature:: Multi-step reaction with 4 steps

1: 94.2 percent / 0.5 N NaOMe(MeOH) / methanol / 3 h / Ambient temperature

2: 85 percent / pyridine / 0.5 h / 0 °C

3: 72.5 percent / BF₃*Et₂O / 2 h / 20 °C

4: HCl / acetic acid; acetic anhydride / 24 h / 0 °C / saturated at -10 deg C, in sealed tube

With pyridine; hydrogenchloride; sodium methylate; boron trifluoride diethyl etherate; In methanol; acetic anhydride; acetic acid;

Reference yield:

: 79365-90-5
1,6-anhydro-β-di-N-acetylchitobiose

: 79365-94-9
2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / pyridine / 0.5 h / 0 °C

2: 72.5 percent / BF₃*Et₂O / 2 h / 20 °C

3: HCl / acetic acid; acetic anhydride / 24 h / 0 °C / saturated at -10 deg C, in sealed tube

With pyridine; hydrogenchloride; boron trifluoride diethyl etherate; In acetic anhydride; acetic acid;

Reference yield:

: 79365-92-7
1,6-di-O-acetyl-3,3',4',6'-tetra-O-benzoyl-α-di-N-acetylchitobiose

: 79365-94-9
2-methyl-<6-O-acetyl-3-O-benzoyl-1,2-dideoxy-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyrano><2,1-d>-2-oxazoline

: 79365-93-8
2-acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-glucopyranosyl)-6-O-acetyl-3-O-benzoyl-2-deoxy-α-D-glucopyranosyl chloride

Guidance literature:: With hydrogenchloride; In acetic anhydride; acetic acid; at 0 ℃; for 24h; Title compound not separated from byproducts; saturated at -10 deg C, in sealed tube;