(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide

Base Information

Chemical Name:(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide
CAS No.:338731-18-3
Molecular Formula:C₂₇H₃₀N₂O₆
Molecular Weight:478.545
Hs Code.:

Synonyms:(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide

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Chemical Property of (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide

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Technology Process of (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide

There total 3 articles about (2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4393-09-3
2,3-dimethoxybenzyl amine

: 338731-26-3
N-2,3-Dimethoxybenzoyl-L-phenyl alanine

: 338731-18-3
(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 21h;
DOI:10.1055/s-2001-11438

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 338731-18-3
(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxybenztriazole; ethyl(dimethylaminopropyl)carbodiimide / dimethylformamide / 17 h / 0 - 20 °C

1.2: aq. NaOH / dimethylformamide / 14 h

2.1: hydroxybenztriazole; ethyl(dimethylaminopropyl)carbodiimide / dimethylformamide / 21 h / 20 °C

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1055/s-2001-11438

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 338731-18-3
(2S)-2-(2,3-Dimethoxyphenyl)carbonyl amino-N-(2,3-dimethoxybenzyl)-3-phenylethylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxybenztriazole; ethyl(dimethylaminopropyl)carbodiimide / dimethylformamide / 17 h / 0 - 20 °C

1.2: aq. NaOH / dimethylformamide / 14 h

2.1: hydroxybenztriazole; ethyl(dimethylaminopropyl)carbodiimide / dimethylformamide / 21 h / 20 °C

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1055/s-2001-11438