Technology Process of C57H74F2N4O10Si2
There total 17 articles about C57H74F2N4O10Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at -78 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere
2: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / Inert atmosphere
3: lithium borohydride; ethanol / ethanol; tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice
4: 1H-imidazole / dichloromethane / 2 h / 0 - 20 °C
5: zinc; formic acid / ethanol / 0.42 h / 20 °C
6: pyridine / dichloromethane / 2 h / -78 °C
With
pyridine; 1H-imidazole; 2,6-dimethylpyridine; lithium borohydride; formic acid; ethanol; sodium carbonate; zinc;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
2: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / Inert atmosphere
2: lithium borohydride; ethanol / ethanol; tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice
3: 1H-imidazole / dichloromethane / 2 h / 0 - 20 °C
4: zinc; formic acid / ethanol / 0.42 h / 20 °C
5: pyridine / dichloromethane / 2 h / -78 °C
With
pyridine; 1H-imidazole; lithium borohydride; formic acid; ethanol; sodium carbonate; zinc;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
1: Suzuki Coupling;