25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt

Base Information

• Chemical Name: 25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt
• CAS No.: 1565870-96-3
• Molecular Formula: C₄₉H₆₁N₄O₁₁*Na
• Molecular Weight: 905.033
• Mol file: 1565870-96-3.mol

Synonyms:25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt

Chemical Property of 25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt

There total 3 articles about 25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3-(4-cinnamylpiperazinyl iminomethyl) rifamycin SV → 25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt (1565870-96-3)

Guidance literature:

With water; sodium hydroxide; In ethanol; for 0.166667h;

Reference yield:

N1-cinnamyl-N4-amino piperazine (41379-00-4) → 25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt (1565870-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / ethanol / 2 h / 20 - 30 °C

2: sodium hydroxide; water / ethanol / 0.17 h

With water; acetic acid; sodium hydroxide; In ethanol;

Reference yield:

3-formylrifamycin SV (13292-22-3) → 25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV sodium salt (1565870-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / ethanol / 2 h / 20 - 30 °C

2: sodium hydroxide; water / ethanol / 0.17 h

With water; acetic acid; sodium hydroxide; In ethanol;

upstream raw materials:

N₁-cinnamyl-N₄-amino piperazine

3-formylrifamycin SV

Downstream raw materials:

25-desacetyl-3-(4-cinnamyl-1-piperazinyl)iminomethyl rifamycin SV