(S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal

Base Information

Chemical Name:(S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal
CAS No.:1071974-88-3
Molecular Formula:C₂₃H₃₆O₄Si
Molecular Weight:404.622
Hs Code.:

Synonyms:(S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal

Chemical Property:

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Technology Process of (S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal

There total 1 articles about (S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1071974-96-3
C₂₃H₃₈O₄Si

: 1071974-88-3
(S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal

Guidance literature:: With pyridine; silica gel; pyridinium chlorochromate; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1021/ol801940r

Reference yield: 40.0%

: 952427-82-6
(1-ethoxypenta-1,3-dienyloxy)trimethylsilane

: 1071974-88-3
(S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal

: 1071974-93-0
C₂₈H₄₂O₅Si

: C₂₈H₄₂O₅Si

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); (R)-tol-BINAP; tetrabutylammonium triphenyldifluorosilicate; In tetrahydrofuran; at 20 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol801940r

Reference yield:

: 901126-38-3
(S)-4-(triisopropylsilyl)but-3-yn-2-yl methanesulfonate

: 1071974-88-3
(S,E)-5-(4-methoxybenzyloxy)-7-((tert-butyldimethylsilyloxy)methyl)octa-2,7-dienal

: (3R,4S,8S,5E)-10-((tert-butyldimethylsilyloxy)methyl)-8-(4-methoxybenzyloxy)-3-methyl-1-(triisopropylsilyl)undeca-5,10-dien-1-yn-4-ol

Guidance literature:: With indium iodide; palladium diacetate; triphenylphosphine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol1011423