meso-tetraphenyl-2-oxa-3-oxoporphyrinatonickel(II)

Base Information

• Chemical Name: meso-tetraphenyl-2-oxa-3-oxoporphyrinatonickel(II)
• CAS No.: 922142-13-0
• Molecular Formula: C₄₃H₂₆N₄NiO₂
• Molecular Weight: 689.395

Synonyms:meso-tetraphenyl-2-oxa-3-oxoporphyrinatonickel(II)

Chemical Property of meso-tetraphenyl-2-oxa-3-oxoporphyrinatonickel(II)

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of meso-tetraphenyl-2-oxa-3-oxoporphyrinatonickel(II)

There total 8 articles about meso-tetraphenyl-2-oxa-3-oxoporphyrinatonickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

meso-tetraphenyl-2,3-dihydroxychlorin + nickel(II) acetate tetrahydrate (6018-89-9) → [meso-tetraphenyl-2,3-dioxoporphyrinato]nickelII (574735-10-7) + [meso-tetraphenyl-2,3-vic-diolchlorinato]nickel(II) + meso-tetraphenyl-2-oxa-3-oxoporphyrinatonickel(II) (922142-13-0) + (2-hydroxy-5,10,15,20-tetraphenylporphyrinato)nickel(II) (112803-38-0)

Guidance literature:

In pyridine; other Radiation; porphyrin, metal salt and pyridine were sealed in a glass tube, microwave power of 300 W, heated from room temp. to 180°C, stirred for 15min, cooled to 50°C; vessel was opened, decanted, TLC (silica gel), UV;

DOI:10.1039/b716181f

Reference yield: 65.0%

[2,4-diformyl-1,5,10,15-tetraphenylchlorophinato]nickel(II) (221911-02-0) → meso-tetraphenyl-2-oxa-3-oxoporphyrinatonickel(II) (922142-13-0) + C43H28N4NiO2 (1167529-51-2)

Guidance literature:

With oxygen; tetraethylammonium hydroxide; In tetrahydrofuran; water; at 20 ℃; Inert atmosphere;

DOI:10.1021/jo9006046

Reference yield: 55.0%

C44H30N4NiO2 (203568-12-1) → [meso-tetraphenyl-3-oxo-2-oxaporphyrinato]Ni(II) (922142-13-0)

Guidance literature:

With potassium permanganate; 18-crown-6 ether; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1021/jo300963m

upstream raw materials:

nickel(II) acetate tetrahydrate

[meso-tetraphenyl-2,3-dioxoporphyrinato]nickel^II

[2,4-diformyl-1,5,10,15-tetraphenylchlorophinato]nickel(II)

C₄₄H₃₀N₄NiO₂

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