3β-benzyloxy-12β-hydroxy-dehydroepiandrosterone

Base Information

Chemical Name:3β-benzyloxy-12β-hydroxy-dehydroepiandrosterone
CAS No.:1198184-74-5
Molecular Formula:C₂₆H₃₄O₃
Molecular Weight:394.554
Hs Code.:

Synonyms:3β-benzyloxy-12β-hydroxy-dehydroepiandrosterone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3β-benzyloxy-12β-hydroxy-dehydroepiandrosterone

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Technology Process of 3β-benzyloxy-12β-hydroxy-dehydroepiandrosterone

There total 2 articles about 3β-benzyloxy-12β-hydroxy-dehydroepiandrosterone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: C₃₃H₄₂N₂O

: 1198184-74-5
3β-benzyloxy-12β-hydroxy-dehydroepiandrosterone

Guidance literature:: C₃₃H₄₂N₂O; With oxygen; copper(II) bis(trifluoromethanesulfonate); sodium L-ascorbate; In methanol; acetone; at 20 - 50 ℃; for 1.58333h;

With water; ethylene diamine tetraacetic acid tetrasodium salt; In methanol; ethyl acetate; acetone; at 20 ℃; for 1h; pH=Ca. 10; Reagent/catalyst; chemoselective reaction;
DOI:10.1021/jacs.5b09463