copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole

Base Information

• Chemical Name: copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole
• CAS No.: 1131806-91-1
• Molecular Formula: C₆₂H₅₉CuN₆O₂S
• Molecular Weight: 1015.8

Synonyms:copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole

Chemical Property of copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole

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Technology Process of copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole

There total 2 articles about copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

para-tert-butylphenol (98-54-4) + copper 10-(4,6-dichloro-2-methylsulfanylpyrimidin-5-yl)-5,15-bis(2,4,6-trimethylphenyl)corrole (948863-58-9) → copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole (1131806-91-1)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 14h;

DOI:10.1039/b819185a

Reference yield: 81.0%

para-tert-butylphenol (98-54-4) + [CuC19H8N4(C6H2(CH3)3)2(C4N2Cl2SCH3)] (948863-58-9) → [CuC19H8N4(C6H2(CH3)3)2(C4N2SCH3(OC6H4C(CH3)3)2)] (1131806-91-1)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 120°C for 14 h;

DOI:10.1039/b819185a

Reference yield: 90.0%

copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole (1131806-91-1) → 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole

Guidance literature:

copper 10-[4,6-bis(4-tert-butylphenoxy)-2-methylsulfanylpyrimidin-5-yl]-5,15-bis(2,4,6-trimethylphenyl)corrole; With tin(II) chloride dihdyrate; In dichloromethane; acetonitrile; at 20 ℃; for 0.166667h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; acetonitrile; at 20 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1039/b819185a

upstream raw materials:

para-tert-butylphenol

[CuC₁₉H₈N₄(C₆H₂(CH₃)3)2(C₄N₂Cl₂SCH₃)]

copper 10-(4,6-dichloro-2-methylsulfanylpyrimidin-5-yl)-5,15-bis(2,4,6-trimethylphenyl)corrole

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