4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate

Base Information

Chemical Name:4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate
CAS No.:139009-73-7
Molecular Formula:C₂₇H₃₅N₃O₇
Molecular Weight:513.591
Hs Code.:

4-acetamidophenyl-N<sup>2</sup>-(tert-butoxycarbonyl)-N<sup>6</sup>-(benzyloxycarbonyl)-L-lysinate

Synonyms:4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate

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Chemical Property of 4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate

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Technology Process of 4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate

There total 1 articles about 4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 2389-45-9
Boc-Lys(Z)-OH

: 103-90-2,8055-08-1
4-acetaminophenol

: 139009-73-7
4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; 1) 0-5 deg C, 1 h, 2) 25 deg C, 3 h;
DOI:10.1016/S0040-4020(01)80998-4

Reference yield: 88.0%

: 139009-73-7
4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate

: 76-05-1
trifluoroacetic acid

: 139009-81-7
(S)-2-Amino-6-benzyloxycarbonylamino-hexanoic acid 4-acetylamino-phenyl ester; compound with trifluoro-acetic acid

Guidance literature:: In water; at 0 - 5 ℃; for 1.5h;
DOI:10.1016/S0040-4020(01)80998-4

Reference yield: 87.0%

: 104-15-4
toluene-4-sulfonic acid

: 139009-73-7
4-acetamidophenyl-N²-(tert-butoxycarbonyl)-N⁶-(benzyloxycarbonyl)-L-lysinate

: 139009-93-1
4-acetamidophenyl-N²-(tert-butoxycarbonyl)-L-lysinate 4-toluenesulfonate

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; at 25 ℃; for 1h; under 2068.6 Torr;
DOI:10.1016/S0040-4020(01)80998-4