PdCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

Base Information

Chemical Name:PdCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2
CAS No.:91410-15-0
Molecular Formula:C₅₀H₄₀Cl₂N₂O₂P₂Pd
Molecular Weight:940.153
Hs Code.:

PdCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2PC<sub>6</sub>H<sub>4</sub>NHC(O)C<sub>6</sub>H<sub>5</sub>)2

Synonyms:PdCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

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Chemical Property of PdCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

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Technology Process of PdCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

There total 1 articles about PdCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: sodium tetrachloropalladate

: 91409-99-3
o-(diphenylphosphino)-N-benzoylaniline

: 91410-15-0
PdCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

Guidance literature:: In acetonitrile; dissolving Pd complex in CH3CN under dry N2; filtration; rapid addn. ofsoln. of ligand in CH3CN to stirred Na2PdCl4 soln.;; filtration after 15 min; washing successively with 3 portions of methanol and (C2H5)2O; drying in vac.; recrystn. from CH2Cl2/CH3OH; elem. anal.;;

Reference yield: 97.0%

: 91410-15-0
PdCl₂((C₆H₅)2PC₆H₄NHC(O)C₆H₅)2

: 99642-35-0
Pd((C₆H₅)2PC₆H₄NC(O)C₆H₅)2

: Pd((C₆H₅)2PC₆H₄NC(O)C₆H₄)((C₆H₅)2PC₆H₄NHC(O)C₆H₅)

: Pd((C₆H₅)2PC₆H₄NC(O)C₆H₅)((C₆H₅)2PC₆H₄NHC(O)C₆H₅)Cl

Guidance literature:: With DABCO; In acetonitrile; Pd complex and DABCO suspended in MeCN, stirred for 3 h; ppt. filtered, washed with acetone, dried in vac.; elem. anal.;
DOI:10.1021/om00133a024