1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Base Information

Chemical Name:1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate
CAS No.:1415043-84-3
Molecular Formula:C₃₂H₃₅FN₂O₈S
Molecular Weight:626.703
Hs Code.:

1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Synonyms:1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

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Chemical Property of 1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

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Technology Process of 1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

There total 8 articles about 1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1415043-08-1
(3-{2-[(4-Fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetic acid

: 99464-83-2
1-chloroethyl cyclohexyl carbonate

: 1415043-84-3
1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: [3-(2,2-dimethyl-4,6-dioxo-[1,3]-dioxan-5-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester

: 1415043-84-3
1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1: ethyl acetate / 2.5 h / Reflux

2: potassium carbonate / chloroform / 20 °C

3: sodium acetate / ethanol / 20 °C

4: acetic anhydride; hypophosphorous acid; water; hydrogen iodide / 96 h / 20 °C

5: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With water; hydrogen iodide; sodium acetate; hypophosphorous acid; acetic anhydride; potassium carbonate; In ethanol; chloroform; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1004293-27-9
2-[(4-fluorophenyl)sulfonyl]benzaldehyde

: 1415043-84-3
1-{[(Cyclohexyloxy)carbonyl]oxy}ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride; hypophosphorous acid; water; hydrogen iodide / 96 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With water; hydrogen iodide; hypophosphorous acid; acetic anhydride; potassium carbonate; In N,N-dimethyl-formamide;