(S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid

Base Information

Chemical Name:(S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid
CAS No.:131196-58-2
Molecular Formula:C₅H₁₀O₂*C₁₉H₂₈N₂O₆
Molecular Weight:482.574
Hs Code.:

Synonyms:(S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid

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Chemical Property of (S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid

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Technology Process of (S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid

There total 5 articles about (S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13650-49-2,184576-63-4
N^δ-(tert-butoxycarbonyl)-L-ornithine

: 131196-58-2
(S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) sodium cyanoborohydride / 1.) methanol, 20 min

2: 1.) sodium bicarbonate / 1.) water, dioxane, 15 min, 2.) 0 deg C, 4 h

3: diethyl ether / 0 °C

4: 96percent formic acid / 4.5 h / 10 °C

With formic acid; sodium cyanoborohydride; sodium hydrogencarbonate; In diethyl ether;
DOI:10.1021/ja00181a035

Reference yield:

: 131196-55-9
δ-N-(tert-butyloxycarbonyl)-α-N-(2,4-dimethoxybenzyl)-L-ornithine

: 131196-58-2
(S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium bicarbonate / 1.) water, dioxane, 15 min, 2.) 0 deg C, 4 h

2: diethyl ether / 0 °C

3: 96percent formic acid / 4.5 h / 10 °C

With formic acid; sodium hydrogencarbonate; In diethyl ether;
DOI:10.1021/ja00181a035

Reference yield:

: 131196-61-7
(S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-tert-butoxycarbonylamino-pentanoic acid

: 131196-58-2
(S)-2-[Allyloxycarbonyl-(2,4-dimethoxy-benzyl)-amino]-5-amino-pentanoic acid methyl ester; compound with 2,2-dimethyl-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 0 °C

2: 96percent formic acid / 4.5 h / 10 °C

With formic acid; In diethyl ether;
DOI:10.1021/ja00181a035