(1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane

Base Information

Chemical Name:(1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane
CAS No.:1186088-69-6
Molecular Formula:C₂₇H₃₉IO₈
Molecular Weight:618.506
Hs Code.:

(1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane

Synonyms:(1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane

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Chemical Property of (1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane

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Technology Process of (1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane

There total 1 articles about (1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1186088-68-5
(1R,3S,4R,5S)-1-[(1R)-2-hydroxy-1-(4-methoxyphenylmethoxy)ethyl]-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane

: 1186088-69-6
(1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo9012546

Reference yield: 50.0%

: 1186088-69-6
(1R,3S,4R,5S)-4-[(1S,2S,3E)-4-iodo-2-methoxy-1-(methoxymethoxy)pent-3-enyl]-3-methoxy-[(1S)-1-(4-methoxyphenylmethoxy)-2-oxoethyl]-7,7-dimethyl-2-oxabicyclo[3.2.0]heptane

: 1186088-71-0
C₂₇H₄₀O₈

: 1186088-70-9
(1R,2R,3S,4E,6S,7S,8R,9S,13S)-3-hydroxy-6,13-dimethoxy-7-(methoxymethoxy)-2-(4-methoxyphenylmethoxy)-4,11,11-trimethyl-12-oxatricyclo[6.3.2.0(1,9)]tridec-4-ene

Guidance literature:: With chromium dichloride; nickel dichloride; In dimethyl sulfoxide; at 20 ℃; for 13h; Inert atmosphere;
DOI:10.1021/jo9012546