1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete

Base Information

Chemical Name:1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete
CAS No.:122768-59-6
Molecular Formula:C₁₆H₃₃NP₂
Molecular Weight:301.392
Hs Code.:

Synonyms:1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete

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Chemical Property of 1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete

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Technology Process of 1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete

There total 1 articles about 1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78129-68-7
2,2-dimethylpropylidynephosphine

: 122768-55-2
(tert-Butylimino)(1,1-diethylpropyl)phosphan

: 122768-59-6
1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete

Guidance literature:: In hexane; at -30 ℃;
DOI:10.1016/S0040-4039(00)95227-4

Reference yield: 96.0%

: 12120-15-9
ethylenebis(triphenylphosphine)platinum⁽⁰⁾

: 122768-59-6
1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete

: 129890-41-1
Pt(PPh₃)2(PCEt₃(N(t-butyl))P=C(t-butyl))

Guidance literature:: In toluene; addn. of the azadiphosphetine soln. to a soln. of the platinum complex, stirring for 24 h; removal of the solvent;
DOI:10.1016/0022-328X(93)83274-Y

Reference yield: 70.0%

: 14694-95-2
Wilkinson's catalyst

: 122768-59-6
1,3-Di-tert-butyl-2-(1,1-diethyl-propyl)-1,2-dihydro-[1,2,4]azadiphosphete

: 129890-43-3
trans-{Rh(PPh₃)2Cl(PCEt₃(N(t-butyl))P=C(t-butyl))}

Guidance literature:: In dichloromethane; addn. of a soln. of the rhodium complex to a soln. of the azadiphosphetine, stirring for 24 h; removal of the solvent, washing with petroleum ether, elem. anal.;
DOI:10.1016/0022-328X(93)83274-Y