5'-deoxy-2',3'-O,O-isopropylidene-5'-[(N-methylcarbamoyl)amino]-N₆-(N-phenylcarbamoyl)adenosine

Base Information

• Chemical Name: 5'-deoxy-2',3'-O,O-isopropylidene-5'-[(N-methylcarbamoyl)amino]-N₆-(N-phenylcarbamoyl)adenosine
• CAS No.: 1092548-22-5
• Molecular Formula: C₂₂H₂₆N₈O₅
• Molecular Weight: 482.499

Synonyms:5'-deoxy-2',3'-O,O-isopropylidene-5'-[(N-methylcarbamoyl)amino]-N₆-(N-phenylcarbamoyl)adenosine

Chemical Property of 5'-deoxy-2',3'-O,O-isopropylidene-5'-[(N-methylcarbamoyl)amino]-N₆-(N-phenylcarbamoyl)adenosine

Chemical Property:

Purity/Quality:

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Technology Process of 5'-deoxy-2',3'-O,O-isopropylidene-5'-[(N-methylcarbamoyl)amino]-N₆-(N-phenylcarbamoyl)adenosine

There total 1 articles about 5'-deoxy-2',3'-O,O-isopropylidene-5'-[(N-methylcarbamoyl)amino]-N₆-(N-phenylcarbamoyl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrophenyl N-methylcarbamate (5819-21-6) + C20H23N7O4 (1092548-27-0) → 5'-deoxy-2',3'-O,O-isopropylidene-5'-[(N-methylcarbamoyl)amino]-N6-(N-phenylcarbamoyl)adenosine (1092548-22-5)

Guidance literature:

With sodium carbonate; In ethyl acetate; for 4h; Inert atmosphere;

DOI:10.1080/15257770903044432

Reference yield: 75.0%

5'-deoxy-2',3'-O,O-isopropylidene-5'-[(N-methylcarbamoyl)amino]-N6-(N-phenylcarbamoyl)adenosine (1092548-22-5) → 5'-deoxy-5'-[(N-methylcarbamoyl)amino]-N6-(N-phenylcarbamoyl)adenosine (1092548-23-6)

Guidance literature:

With water; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1080/15257770903044432

upstream raw materials:

4-nitrophenyl N-methylcarbamate

C₂₀H₂₃N₇O₄

Downstream raw materials:

5'-deoxy-5'-[(N-methylcarbamoyl)amino]-N₆-(N-phenylcarbamoyl)adenosine

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