3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester

Base Information

Chemical Name:3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester
CAS No.:915128-45-9
Molecular Formula:C₁₇H₂₈BNO₄
Molecular Weight:321.225
Hs Code.:

Synonyms:3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester

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Chemical Property of 3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester

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Technology Process of 3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester

There total 1 articles about 3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113999-02-3
ethyl 3,4-diethyl-5-iodo-1H-pyrrole-2-carboxylate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 915128-45-9
3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester

: 97336-41-9
ethyl 3,4-diethyl-1H-pyrrole-2-carboxylate

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 60 ℃; for 3h; Further Variations:; Catalysts; Reagents; Reaction partners; times; Product distribution;
DOI:10.1016/j.tetlet.2006.08.098

Reference yield: 92.0%

: 915128-45-9
3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester

: 3001-15-8
4,4'-diiodobiphenyl

: 4,4’-bis(5-carboethoxy-3,4-diethylpyrrol-2-yl)biphenyl

Guidance literature:: With potassium carbonate; triphenylphosphine; palladium diacetate; In water; N,N-dimethyl-formamide; at 80 - 90 ℃; for 5h;
DOI:10.1016/j.tetlet.2006.08.098

Reference yield: 81.0%

: 915128-45-9
3,4-diethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrol-2-ylcarboxylic acid ethyl ester

: 615-42-9
1,2-Diiodobenzene

: C₂₈H₃₆N₂O₄

Guidance literature:: With potassium carbonate; triphenylphosphine; palladium diacetate; In water; N,N-dimethyl-formamide; at 80 - 90 ℃; for 24h;
DOI:10.1016/j.tetlet.2006.08.098