1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate

Base Information

Chemical Name:1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate
CAS No.:1431326-47-4
Molecular Formula:C₂₄H₃₇NO₄
Molecular Weight:403.562
Hs Code.:

Synonyms:1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate

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Chemical Property of 1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate

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Technology Process of 1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate

There total 2 articles about 1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.1%

: 1431326-46-3
tert-butyl cyclohexyl(2-hydroxypropyl)carbamate

: 938-18-1
mesitylene-2-carboxylic acid chloride

: 1431326-47-4
1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate

Guidance literature:: In toluene; at 20 ℃; for 16h;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1431326-47-4
1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 0.17 h / 0 - 10 °C

1.2: 0.25 h / 0 - 20 °C

2.1: triethylamine / tetrahydrofuran / 6 h / 0 - 20 °C

3.1: toluene / 16 h / 20 °C

With triethylamine; In tetrahydrofuran; ethanol; toluene;

Reference yield: 76.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1431326-47-4
1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate

: 1431326-48-5
1-(cyclohexyl(methyl)amino)propan-2-yl-2,4,6-trimethylbenzoate

Guidance literature:: 1-((tert-butoxycarbonyl)(cyclohexyl)amino)propan-2-yl 2,4,6-trimethylbenzoate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

formaldehyd; With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 16h;

With sodium hydroxide; In 1,4-dioxane; dichloromethane; water;