sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate

Base Information

Chemical Name:sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate
CAS No.:1304513-15-2
Molecular Formula:C₁₆H₂₀NO₈*Na
Molecular Weight:377.326
Hs Code.:

Synonyms:sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate

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Chemical Property of sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate

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Technology Process of sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate

There total 3 articles about sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1304513-22-1
C₂₂H₂₇NO₁₁

: 1304513-15-2
sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 1h;
DOI:10.1039/c0mb00206b

Reference yield:

: 4049-33-6
tetra-O-acetyl-β-D-xylopyranose

: 1304513-15-2
sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: palladium on activated charcoal; hydrogen; trifluoroacetic acid / methanol; ethyl acetate / 18 h / 20 °C

3: pyridine / 18 h / 20 °C

4: methanol; sodium methylate / 1 h / 20 °C

With pyridine; methanol; palladium on activated charcoal; boron trifluoride diethyl etherate; hydrogen; sodium methylate; trifluoroacetic acid; In methanol; dichloromethane; ethyl acetate;
DOI:10.1039/c0mb00206b

Reference yield:

: 1304513-16-3
2-cyanoethyl β-D-2,3,4-tri-O-acetyl-xylopyranoside

: 1304513-15-2
sodium N-[O-(β-D-xylopyranosyl)-3-hydroxypropyl]-phthalamate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on activated charcoal; hydrogen; trifluoroacetic acid / methanol; ethyl acetate / 18 h / 20 °C

2: pyridine / 18 h / 20 °C

3: methanol; sodium methylate / 1 h / 20 °C

With pyridine; methanol; palladium on activated charcoal; hydrogen; sodium methylate; trifluoroacetic acid; In methanol; ethyl acetate;
DOI:10.1039/c0mb00206b