2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester

Base Information

Chemical Name:2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester
CAS No.:183549-49-7
Molecular Formula:C₁₈H₂₄O₄S
Molecular Weight:336.452
Hs Code.:

Synonyms:2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester

Suppliers and Price of 2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester

There total 5 articles about 2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21673-18-7
methyl 2-(phenylthio)propanoate

: 183549-49-7
2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: SO₂Cl₂ / CH₂Cl₂ / 0 deg C, then RT

2: 94 percent / toluene / 200 °C / 12 Torr

3: 90 percent / m-chloroperbenzoic acid

4: 1.) CuBr / 1.) ether, hexane, -20 deg C, 20 min; 2.) ether, -20 deg C, 1 h; 3.) ether, -78 deg C, 1 h

With sulfuryl dichloride; 3-chloro-benzenecarboperoxoic acid; copper(I) bromide; In dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)87361-0

Reference yield:

: 85908-43-6
chloro-2 phenylthio-2 propionate de methyle

: 183549-49-7
2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / toluene / 200 °C / 12 Torr

2: 90 percent / m-chloroperbenzoic acid

3: 1.) CuBr / 1.) ether, hexane, -20 deg C, 20 min; 2.) ether, -20 deg C, 1 h; 3.) ether, -78 deg C, 1 h

With 3-chloro-benzenecarboperoxoic acid; copper(I) bromide; In toluene;
DOI:10.1016/S0040-4020(01)87361-0

Reference yield:

: 108-98-5
thiophenol

: 183549-49-7
2-Benzenesulfinyl-3-(2,2-dimethyl-6-oxo-cyclohexyl)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / Et₃N / diethyl ether / 24 h / Heating

2: SO₂Cl₂ / CH₂Cl₂ / 0 deg C, then RT

3: 94 percent / toluene / 200 °C / 12 Torr

4: 90 percent / m-chloroperbenzoic acid

5: 1.) CuBr / 1.) ether, hexane, -20 deg C, 20 min; 2.) ether, -20 deg C, 1 h; 3.) ether, -78 deg C, 1 h

With sulfuryl dichloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; copper(I) bromide; In diethyl ether; dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)87361-0