1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

Base Information

Chemical Name:1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a
CAS No.:66065-92-7
Molecular Formula:C₂₈H₃₉Cl₉N₄O₁₄
Molecular Weight:974.713
Hs Code.:

1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C<sub>1a</sub>

Synonyms:1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

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Chemical Property of 1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

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Technology Process of 1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

There total 1 articles about 1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 66065-87-0
3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

: 66065-92-7
1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

Guidance literature:: With sulfuric acid; 3,5-di-tert-butyl-o-benzoquinone; In methanol; at 25 ℃; for 34h; pH = 3;
DOI:10.1039/P19810002168

Reference yield:

: 66065-92-7
1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

: C₃₀H₄₃Cl₉N₄O₁₅

Guidance literature:: With sulfuric acid; sodium cyanoborohydride; In methanol; at 25 ℃; for 18h; pH = 3;
DOI:10.1039/P19810002168

Reference yield:

: 66065-92-7
1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

: 66065-96-1,66101-46-0
1-deamino-1-hydroxygentamicin C_1a

Guidance literature:: Multi-step reaction with 2 steps

1: 1M-sulphuric acid, sodium cyanoborohydride / methanol / 18 h / 25 °C / pH = 3

2: 7 percent / acetic acid, zinc / methanol / 3 h / Heating

With sulfuric acid; sodium cyanoborohydride; acetic acid; zinc; In methanol;
DOI:10.1039/P19810002168