methyl (E)-5,6-dideoxy-2,3-O-isopropylidene-6-phenyl-β-D-ribo-hex-5-enofuranoside

Base Information

Chemical Name:methyl (E)-5,6-dideoxy-2,3-O-isopropylidene-6-phenyl-β-D-ribo-hex-5-enofuranoside
CAS No.:1091627-36-9
Molecular Formula:C₁₆H₂₀O₄
Molecular Weight:276.332
Hs Code.:

Synonyms:methyl (E)-5,6-dideoxy-2,3-O-isopropylidene-6-phenyl-β-D-ribo-hex-5-enofuranoside

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Chemical Property of methyl (E)-5,6-dideoxy-2,3-O-isopropylidene-6-phenyl-β-D-ribo-hex-5-enofuranoside

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Technology Process of methyl (E)-5,6-dideoxy-2,3-O-isopropylidene-6-phenyl-β-D-ribo-hex-5-enofuranoside

There total 2 articles about methyl (E)-5,6-dideoxy-2,3-O-isopropylidene-6-phenyl-β-D-ribo-hex-5-enofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1091627-35-8
methyl 5-benzylsulfonyl-5-deoxy-2,3-O-isopropylidene-β-D-ribofuranoside

: 1091627-36-9
methyl (E)-5,6-dideoxy-2,3-O-isopropylidene-6-phenyl-β-D-ribo-hex-5-enofuranoside

Guidance literature:: With alumina-supported potassium hydroxide; dibromodifluoromethane; In dichloromethane; butan-1-ol; at 0 - 20 ℃;
DOI:10.1016/j.carres.2008.08.010

Reference yield: 35.0%

: C₉H₁₄O₆

: 536-74-3
phenylacetylene

: 1091627-36-9
methyl (E)-5,6-dideoxy-2,3-O-isopropylidene-6-phenyl-β-D-ribo-hex-5-enofuranoside

: C₁₆H₂₀O₄

Guidance literature:: With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; (1R,2R)-1,2-diaminocyclohexane; cesium acetate; copper diacetate; In N,N-dimethyl acetamide; at 20 ℃; for 24h; Overall yield = 50 percent; diastereoselective reaction; Irradiation;
DOI:10.1021/acscatal.0c01742