(3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone

Base Information

Chemical Name:(3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone
CAS No.:1431501-02-8
Molecular Formula:C₂₆H₃₆N₂O₅S
Molecular Weight:488.648
Hs Code.:

Synonyms:(3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone

Chemical Property:

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Technology Process of (3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone

There total 10 articles about (3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxybenzoic acid

: 1431501-02-8
(3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In 1,4-dioxane; N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 51522-07-7
3-methylsulphonyl-4-chlorobenzoic acid

: 1431501-02-8
(3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid; nitric acid / 1 h / 0 - 110 °C

2.1: sodium hydrogencarbonate / water / 85 °C

3.1: thionyl chloride / 60 °C

4.1: ammonium chloride; iron / water; ethanol / 2.25 h / 85 °C

5.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

6.1: lithium hydroxide / methanol; tetrahydrofuran / 2 h

7.1: trifluoroacetic acid / acetonitrile / 0.5 h / 0 °C

7.2: 0 - 20 °C

8.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide; 1,4-dioxane / 20 °C

With thionyl chloride; sulfuric acid; nitric acid; sodium tris(acetoxy)borohydride; iron; sodium hydrogencarbonate; ammonium chloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 2494-79-3
4-chloro-3-(chlorosulfonyl)benzoic acid

: 1431501-02-8
(3-(dibutylamino)-5-(methylsulfonyl)-4-phenoxyphenyl)(4-morpholinyl)methanone

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium sulfite / water / 3 h / 0 - 20 °C

2.1: sodium hydroxide / water; methanol / 72 h / 20 °C

3.1: sulfuric acid; nitric acid / 1 h / 0 - 110 °C

4.1: sodium hydrogencarbonate / water / 85 °C

5.1: thionyl chloride / 60 °C

6.1: ammonium chloride; iron / water; ethanol / 2.25 h / 85 °C

7.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

8.1: lithium hydroxide / methanol; tetrahydrofuran / 2 h

9.1: trifluoroacetic acid / acetonitrile / 0.5 h / 0 °C

9.2: 0 - 20 °C

10.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide; 1,4-dioxane / 20 °C

With thionyl chloride; sulfuric acid; nitric acid; sodium tris(acetoxy)borohydride; iron; sodium hydrogencarbonate; ammonium chloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; lithium hydroxide; sodium sulfite; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;