Technology Process of 3,9-bis(4-(hexyloxy)phenyl)indolizino[6,5,4,3-ija]quinoline
There total 4 articles about 3,9-bis(4-(hexyloxy)phenyl)indolizino[6,5,4,3-ija]quinoline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
indium(III) chloride;
In
toluene;
at 100 ℃;
for 24h;
Inert atmosphere;
DOI:10.1002/anie.201205007
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran; ethylbenzene; diethyl ether / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: dichloro bis(acetonitrile) palladium(II); copper(l) iodide; tri-tert-butyl phosphine; diisopropylamine / 1,4-dioxane; toluene / 20 °C / Inert atmosphere
3.1: indium(III) chloride / toluene / 24 h / 100 °C / Inert atmosphere
With
indium(III) chloride; dichloro bis(acetonitrile) palladium(II); copper(l) iodide; tri-tert-butyl phosphine; diisopropylamine; lithium diisopropyl amide;
In
tetrahydrofuran; 1,4-dioxane; diethyl ether; n-heptane; ethylbenzene; toluene;
DOI:10.1002/anie.201205007
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloro bis(acetonitrile) palladium(II); copper(l) iodide; tri-tert-butyl phosphine; diisopropylamine / 1,4-dioxane; toluene / 20 °C / Inert atmosphere
2: indium(III) chloride / toluene / 24 h / 100 °C / Inert atmosphere
With
indium(III) chloride; dichloro bis(acetonitrile) palladium(II); copper(l) iodide; tri-tert-butyl phosphine; diisopropylamine;
In
1,4-dioxane; toluene;
DOI:10.1002/anie.201205007
