(R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine

Base Information

Chemical Name:(R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine
CAS No.:725270-16-6
Molecular Formula:C₂₈H₃₆Cl₂N₂O₂
Molecular Weight:503.512
Hs Code.:

Synonyms:(R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine

Suppliers and Price of (R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine

Chemical Property:

Purity/Quality:

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Technology Process of (R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine

There total 3 articles about (R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 135395-82-3
2-hydroxy-3-tert-butyl-5-chloro-benzaldehyde

: 725270-16-6
(R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine

Guidance literature:: In ethanol; for 2h; Reflux;
DOI:10.1021/ja2016813

Reference yield:

: 24623-65-2
3-tert-butyl-2-hydroxybenzaldehyde

: 725270-16-6
(R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: iron(III) chloride; sulfuryl dichloride / 24 h / 20 °C

2: ethanol / 2 h / Reflux

With iron(III) chloride; sulfuryl dichloride; In ethanol;
DOI:10.1021/ja2016813

Reference yield:

: 135395-82-3
2-hydroxy-3-tert-butyl-5-chloro-benzaldehyde

: 32044-22-7,39961-95-0
(1R,2R)-1,2-diaminocyclohexane tartrate

: 725270-16-6
(R,R)-N,N'-bis(3-tert-butyl-5-chlorosalicylidene)-1,2-cyclohexanediamine

Guidance literature:: (1R,2R)-1,2-diaminocyclohexane tartrate; With potassium carbonate; In ethanol; water; for 1.16h; Reflux; Inert atmosphere;

2-hydroxy-3-tert-butyl-5-chloro-benzaldehyde; In ethanol; water; for 2.5h; Inert atmosphere; Reflux;
DOI:10.1039/c5nj00469a