O-methyl (3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

Base Information

Chemical Name:O-methyl (3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate
CAS No.:646536-80-3
Molecular Formula:C₃₃H₄₀O₂SiSn
Molecular Weight:615.475
Hs Code.:

Synonyms:O-methyl (3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

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Chemical Property of O-methyl (3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

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Technology Process of O-methyl (3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

There total 1 articles about O-methyl (3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 181478-00-2
methyl 2-(prop-2-yn-1-yl)pent-4-ynoate

: 185962-47-4
tert-butyldimethylsilyl triphenylstannane

: 646536-80-3
O-methyl (3Z,4Z)-3-[(tert-butyldimethylsilyl)methylene]-4-[(triphenylstannyl)-methylene]cyclopentane carboxylate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In benzene; stirring of soln. of O-methyl-2-(2-propynyl)-4-pentynoate, (tert-butyldimethylsilyl)-triphenylstannane, Pd2(dba)3 and tris-(pentafluorophenyl)phosphine in benzene at room temp. for 15 h (J. Am. Chem. Soc. 2000, 122,8579); evapn. of solvent, chromy. on silica gel (hexane/diethyl ether: 95:5; 90:10);
DOI:10.1021/ja035136m