[bis(triphenylphosphoranylidene)ammonium][Ni(SC₄H₃S)(P(o-C₆H₄S)3)]

Base Information

• Chemical Name: [bis(triphenylphosphoranylidene)ammonium][Ni(SC₄H₃S)(P(o-C₆H₄S)3)]
• CAS No.: 738585-45-0
• Molecular Formula: C₂₂H₁₅NiPS₅*C₃₆H₃₀NP₂
• Molecular Weight: 1067.94

Synonyms:[bis(triphenylphosphoranylidene)ammonium][Ni(SC₄H₃S)(P(o-C₆H₄S)3)]

Chemical Property of [bis(triphenylphosphoranylidene)ammonium][Ni(SC₄H₃S)(P(o-C₆H₄S)3)]

Chemical Property:

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Technology Process of [bis(triphenylphosphoranylidene)ammonium][Ni(SC₄H₃S)(P(o-C₆H₄S)3)]

There total 1 articles about [bis(triphenylphosphoranylidene)ammonium][Ni(SC₄H₃S)(P(o-C₆H₄S)3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

[bis(triphenylphosphoranylidene)ammonium][Ni(2-SC4H3S)(P(o-C6H4S)2(o-C6H4SH))] (738585-41-6) → [bis(triphenylphosphoranylidene)ammonium][Ni(SC4H3S)(P(o-C6H4S)3)] (738585-45-0)

Guidance literature:

With oxygen; In tetrahydrofuran; byproducts: H2O; under N2; dry O2 purged through THF soln. of Ni complex at 0°C; stirred at 0°C for 15 min; pptd. by adding hexane; elem. anal.;

DOI:10.1021/ja048568l

upstream raw materials:

[bis(triphenylphosphoranylidene)ammonium][Ni(2-SC₄H₃S)(P(o-C₆H₄S)2(o-C₆H₄SH))]

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