3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate

Base Information

Chemical Name:3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate
CAS No.:321907-90-8
Molecular Formula:C₁₈H₂₆O₈
Molecular Weight:370.4
Hs Code.:

Synonyms:3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate

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Chemical Property of 3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate

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Technology Process of 3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate

There total 4 articles about 3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3-(4-Methoxyphenyl)propyl methyl 2,3-di-O-benzyl-4-O-methyl-α-D-glucopyranosiduronate

: 321907-90-8
3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; ethanol; at 20 ℃; for 24h;
DOI:10.1135/cccc20001609

Reference yield:

: 5406-18-8
3-(p-methoxyphenyl)-1-propanol

: 321907-90-8
3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / DCC; pyridine / CH₂Cl₂ / 5 h / 20 °C

2: 100 percent / H₂ / 10 percent Pd/C / ethanol; methanol / 24 h / 20 °C

With pyridine; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1135/cccc20001609

Reference yield:

: 51433-17-1
Methyl 2,3-di-O-benzyl-4-O-methyl-α-D-glucopyranoside

: 321907-90-8
3-(4-Methoxyphenyl)propyl methyl 4-O-methyl-α-D-glucopyranosiduronate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / TEMPO; Bu₄NBr; aq. NaOCl / NaHCO₃; KBr / CH₂Cl₂ / 0.5 h / 0 °C

2: 78 percent / DCC; pyridine / CH₂Cl₂ / 5 h / 20 °C

3: 100 percent / H₂ / 10 percent Pd/C / ethanol; methanol / 24 h / 20 °C

With pyridine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; tetrabutylammomium bromide; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; sodium hydrogencarbonate; potassium bromide; In methanol; ethanol; dichloromethane;
DOI:10.1135/cccc20001609