3,4,5-triheptyloxybenzoic hydrazide

Base Information

• Chemical Name: 3,4,5-triheptyloxybenzoic hydrazide
• CAS No.: 956401-93-7
• Molecular Formula: C₂₈H₅₀N₂O₄
• Molecular Weight: 478.716
• Mol file: 956401-93-7.mol

Synonyms:3,4,5-triheptyloxybenzoic hydrazide

Chemical Property of 3,4,5-triheptyloxybenzoic hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4,5-triheptyloxybenzoic hydrazide

There total 4 articles about 3,4,5-triheptyloxybenzoic hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5-triheptyloxybenzoic acid methyl ester → 3,4,5-triheptyloxybenzoic hydrazide (956401-93-7)

Guidance literature:

With hydrazine; In ethanol; for 12h; Heating;

DOI:10.1039/a800657a

Reference yield:

ethyl 3,4,5-tris(heptyloxy)benzoate (1070380-33-4) → 3,4,5-triheptyloxybenzoic hydrazide (956401-93-7)

Guidance literature:

With hydrazine hydrate; In ethanol; for 40h; Heating;

DOI:10.1016/j.tet.2007.09.028

Reference yield:

1-Bromoheptane (629-04-9) → 3,4,5-triheptyloxybenzoic hydrazide (956401-93-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃, KI / acetone / 72 h / Heating

2: NH₂NH₂ / ethanol / 12 h / Heating

With potassium carbonate; potassium iodide; hydrazine; In ethanol; acetone;

DOI:10.1039/a800657a

upstream raw materials:

ethyl 3,4,5-tris(heptyloxy)benzoate

1-Bromoheptane

methyl galloate

Downstream raw materials:

C₇₀H₁₁₀N₄O₁₄