C₃₅H₃₈O₂S

Base Information

Chemical Name:C₃₅H₃₈O₂S
CAS No.:1427470-00-5
Molecular Formula:C₃₅H₃₈O₂S
Molecular Weight:522.752
Hs Code.:

C<sub>35</sub>H<sub>38</sub>O<sub>2</sub>S

Synonyms:C₃₅H₃₈O₂S

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Chemical Property of C₃₅H₃₈O₂S

Chemical Property:

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Technology Process of C₃₅H₃₈O₂S

There total 12 articles about C₃₅H₃₈O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₂H₄₄O₂S

: 1427470-00-5
C₃₅H₃₈O₂S

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 90 ℃; for 4h; Reflux;

Reference yield:

: 578-57-4
2-bromoanisole

: 1427470-00-5
C₃₅H₃₈O₂S

Guidance literature:: Multi-step reaction with 12 steps

1.1: aluminum (III) chloride / dichloromethane / 2 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene / toluene / 3 h / Inert atmosphere; Reflux

3.1: potassium tert-butylate / tetrahydrofuran / 1 h

4.1: sodium acetate / toluene / 3 h / Reflux

5.1: sodium hydroxide; water / methanol / 3 h / Reflux

6.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C

7.1: sodium hydroxide / water; isopropyl alcohol / 3 h / Reflux

8.1: triethylamine; diphenyl phosphoryl azide / toluene / 2 h / 20 °C

8.2: 2 h / 70 °C

8.3: 6 h / Reflux

9.1: sodium nitrite; hydrogenchloride / water; acetonitrile / 0.5 h / 0 - 5 °C

9.2: 5 h / 20 °C

10.1: n-butyllithium / toluene; hexane / 0.5 h / -30 °C

10.2: 3 h / 0 °C

11.1: camphor-10-sulfonic acid / toluene / 0.5 h / Reflux

12.1: toluene-4-sulfonic acid / toluene / 4 h / 90 °C / Reflux

With hydrogenchloride; aluminum (III) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; diphenyl phosphoryl azide; camphor-10-sulfonic acid; potassium tert-butylate; water; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene; acetonitrile;

Reference yield:

: 116413-49-1
(3-bromo-4-methoxyphenyl)-phenylmethanone

: 1427470-00-5
C₃₅H₃₈O₂S

Guidance literature:: Multi-step reaction with 11 steps

1.1: N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene / toluene / 3 h / Inert atmosphere; Reflux

2.1: potassium tert-butylate / tetrahydrofuran / 1 h

3.1: sodium acetate / toluene / 3 h / Reflux

4.1: sodium hydroxide; water / methanol / 3 h / Reflux

5.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C

6.1: sodium hydroxide / water; isopropyl alcohol / 3 h / Reflux

7.1: triethylamine; diphenyl phosphoryl azide / toluene / 2 h / 20 °C

7.2: 2 h / 70 °C

7.3: 6 h / Reflux

8.1: sodium nitrite; hydrogenchloride / water; acetonitrile / 0.5 h / 0 - 5 °C

8.2: 5 h / 20 °C

9.1: n-butyllithium / toluene; hexane / 0.5 h / -30 °C

9.2: 3 h / 0 °C

10.1: camphor-10-sulfonic acid / toluene / 0.5 h / Reflux

11.1: toluene-4-sulfonic acid / toluene / 4 h / 90 °C / Reflux

With hydrogenchloride; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; diphenyl phosphoryl azide; camphor-10-sulfonic acid; potassium tert-butylate; water; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; hexane; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene; acetonitrile;