C₅₃H₆₈O₉Si

Base Information

Chemical Name:C₅₃H₆₈O₉Si
CAS No.:927662-07-5
Molecular Formula:C₅₃H₆₈O₉Si
Molecular Weight:877.203
Hs Code.:

C<sub>53</sub>H<sub>68</sub>O<sub>9</sub>Si

Synonyms:C₅₃H₆₈O₉Si

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Chemical Property of C₅₃H₆₈O₉Si

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Technology Process of C₅₃H₆₈O₉Si

There total 14 articles about C₅₃H₆₈O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 927662-05-3
C₅₅H₇₂O₉Si

: 927662-06-4
C₅₃H₆₈O₉Si

: 927662-07-5
C₅₃H₆₈O₉Si

Guidance literature:: ruthenium ethylidene complex; In toluene; at 100 ℃;
DOI:10.3987/COM-06-S(O)23

Reference yield:

: C₁₀H₁₆O₅

: 927662-07-5
C₅₃H₆₈O₉Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: NaHMDS / tetrahydrofuran; dimethylformamide / 2 h / 20 °C

1.2: p-TSOH*H₂O / methanol; H₂O; tetrahydrofuran / 0.75 h / 20 °C

1.3: 86 percent / 2,6-lutidine / tetrahydrofuran; dimethylformamide / 0.17 h / 0 °C

2.1: 9-BBN / tetrahydrofuran / 3 h / 20 °C / sonication

2.2: H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 1 h / 20 °C

2.3: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.58 h / 20 °C

3.1: 78 percent / Sc(OTf)3 / benzene / 14 h / 20 °C

4.1: Sc(OTf)3 / CH₂Cl₂ / 9.5 h / 20 °C

4.2: 92 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

5.1: 2-nitrobenzeneselenide; Bu₃P / tetrahydrofuran / 0.42 h / 20 °C

5.2: 77 percent / H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 3.5 h / 45 °C

6.1: 89 percent / DIBAL-H / CH₂Cl₂ / 0.5 h / -78 °C

7.1: 76 percent / MeLi / tetrahydrofuran / 1 h / -78 - 20 °C

8.1: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

9.1: 67 percent / ruthenium ethylidene complex / toluene / 100 °C

With 9-borabicyclo[3.3.1]nonane dimer; tributylphosphine; methyllithium; sodium hexamethyldisilazane; diisobutylaluminium hydride; Dess-Martin periodane; scandium tris(trifluoromethanesulfonate); ruthenium ethylidene complex; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.3987/COM-06-S(O)23

Reference yield:

: 927661-96-9
C₂₇H₃₈O₄Si

: 927662-07-5
C₅₃H₆₈O₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 9-BBN / tetrahydrofuran / 3 h / 20 °C / sonication

1.2: H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 1 h / 20 °C

1.3: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.58 h / 20 °C

2.1: 78 percent / Sc(OTf)3 / benzene / 14 h / 20 °C

3.1: Sc(OTf)3 / CH₂Cl₂ / 9.5 h / 20 °C

3.2: 92 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

4.1: 2-nitrobenzeneselenide; Bu₃P / tetrahydrofuran / 0.42 h / 20 °C

4.2: 77 percent / H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 3.5 h / 45 °C

5.1: 89 percent / DIBAL-H / CH₂Cl₂ / 0.5 h / -78 °C

6.1: 76 percent / MeLi / tetrahydrofuran / 1 h / -78 - 20 °C

7.1: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

8.1: 67 percent / ruthenium ethylidene complex / toluene / 100 °C

With 9-borabicyclo[3.3.1]nonane dimer; tributylphosphine; methyllithium; diisobutylaluminium hydride; Dess-Martin periodane; scandium tris(trifluoromethanesulfonate); ruthenium ethylidene complex; In tetrahydrofuran; dichloromethane; toluene; benzene;
DOI:10.3987/COM-06-S(O)23