1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline

Base Information

Chemical Name:1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline
CAS No.:1310876-25-5
Molecular Formula:C₂₀H₂₀ClN₃O₃
Molecular Weight:385.85
Hs Code.:

Synonyms:1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline

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Chemical Property of 1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline

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Technology Process of 1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline

There total 1 articles about 1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 3382-18-1
6,7-dimethoxy-3,4-dihydro-isoquinoline

: 18247-78-4,1338563-31-7
2-oxo-N-(4-chlorophenyl)propanehydrazonoyl chloride

: 1310876-25-5
1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline

Guidance literature:: With chitosan; In ethanol; at 80 ℃; for 0.166667h; under 8400.84 Torr; Microwave irradiation;
DOI:10.1515/znb-2011-0313

Reference yield: 79.0%

: 1310876-25-5
1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 1310876-28-8
(E)-1-(8,9-dimethoxy-1-(4-chlorophenyl)-1,5,6,10b-tetrahydro[1,2,4]triazolo[3,4-a]iso-quinolin-3-yl)-3-(dimethylamino)prop-2-en-1-one

Guidance literature:: for 4h; Reflux;
DOI:10.1515/znb-2011-0313

Reference yield:

: 1310876-25-5
1,5,6,10b-tetrahydro-1-(4-chlorophenyl)-3-acetyl-8,9-dimethoxy[1,2,4]triazolo-[3,4-a]isoquinoline

: 1310876-35-7
1-[4-(8,9-dimethoxy-1-(4-chlorophenyl)-1,5,6,10b-tetrahydro[1,2,4]triazolo[3,4-a]iso-quinoline-3-carbonyl)-1-phenyl-1H-pyrazol-3-yl]ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 4 h / Reflux

2: chitosan / ethanol / 0.17 h / 80 °C / 8400.84 Torr / Microwave irradiation

With chitosan; In ethanol;
DOI:10.1515/znb-2011-0313