(4S,5R)-2,2-di-tert-butyl-4-(((2S,3R)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane

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Chemical Name:(4S,5R)-2,2-di-tert-butyl-4-(((2S,3R)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane
CAS No.:1338565-65-3
Molecular Formula:C₃₈H₇₀O₈SSi₃
Molecular Weight:771.291
Hs Code.:

(4S,5R)-2,2-di-tert-butyl-4-(((2S,3R)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane

Synonyms:(4S,5R)-2,2-di-tert-butyl-4-(((2S,3R)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane

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Chemical Property of (4S,5R)-2,2-di-tert-butyl-4-(((2S,3R)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane

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Technology Process of (4S,5R)-2,2-di-tert-butyl-4-(((2S,3R)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane

There total 1 articles about (4S,5R)-2,2-di-tert-butyl-4-(((2S,3R)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: cis-3-((2R,3S)-3-(tert-butyldimethylsiloxy)tetrahydropyran-2-yl)-1,2-epoxypropan-1-yl phenyl sulfone

: 391235-70-4
(4S,5R)-2,2-di-tert-butyl-5-triethylsiloxy-1,3-dioxa-2-silacyclohexane-4-methyl trifluoromethanesulfonate

: 1338565-65-3
(4S,5R)-2,2-di-tert-butyl-4-(((2S,3R)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane

: 1338565-64-2
(4S,5R)-2,2-di-tert-butyl-4-(((2R,3S)-3-(((2R,3S)-3-((tert-butyldimethylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-2-(phenylsulfonyl)oxiran-2-yl)methyl)-5-((triethylsilyl)oxy)-1,3,2-dioxasilinane

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; hexane; at -100 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1021/ol202467z