undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate

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Chemical Name:undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate
CAS No.:1443687-80-6
Molecular Formula:C₃₆H₅₆N₄O₄
Molecular Weight:608.865
Hs Code.:

Synonyms:undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate

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Chemical Property of undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate

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Technology Process of undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate

There total 4 articles about undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112-64-1
tetradecanoyl chloride

: 1443687-80-6
undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / acetonitrile / 2.25 h / 0 - 10 °C

1.2: 16 h / 20 °C

2.1: potassium tert-butylate / ethanol / 72 h / Reflux

3.1: triethylamine / tetrahydrofuran / 18 h / Reflux

4.1: sodium hydroxide / ethanol / 18 h / 70 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / chloroform / 72 h / Reflux

With dmap; potassium tert-butylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; chloroform; acetonitrile;
DOI:10.1039/c2ra22715k

Reference yield:

: 2-amino-4-hydroxy-6-tridecylpyrimidine

: 1443687-80-6
undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 18 h / Reflux

2: sodium hydroxide / ethanol / 18 h / 70 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / chloroform / 72 h / Reflux

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1039/c2ra22715k

Reference yield:

: 1443687-75-9
ethyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido)benzoate

: 1443687-80-6
undec-10-enyl 4-(3-(4-oxo-6-tridecyl-1,4-dihydropyrimidin-2-yl)ureido) benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 18 h / 70 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / chloroform / 72 h / Reflux

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In ethanol; chloroform;
DOI:10.1039/c2ra22715k