(1S,2R,3S,5S)-2-benzyloxy-3-benzyloxymethyl-5-(trimethylsilylethynyl)cyclopentanol

Base Information

Chemical Name:(1S,2R,3S,5S)-2-benzyloxy-3-benzyloxymethyl-5-(trimethylsilylethynyl)cyclopentanol
CAS No.:1005006-72-3
Molecular Formula:C₂₅H₃₂O₃Si
Molecular Weight:408.613
Hs Code.:

Synonyms:(1S,2R,3S,5S)-2-benzyloxy-3-benzyloxymethyl-5-(trimethylsilylethynyl)cyclopentanol

Suppliers and Price of (1S,2R,3S,5S)-2-benzyloxy-3-benzyloxymethyl-5-(trimethylsilylethynyl)cyclopentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,3S,5S)-2-benzyloxy-3-benzyloxymethyl-5-(trimethylsilylethynyl)cyclopentanol

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Technology Process of (1S,2R,3S,5S)-2-benzyloxy-3-benzyloxymethyl-5-(trimethylsilylethynyl)cyclopentanol

There total 1 articles about (1S,2R,3S,5S)-2-benzyloxy-3-benzyloxymethyl-5-(trimethylsilylethynyl)cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1005006-71-2
(1S,2R,3S,4S)-1-benzyloxymethyl-2-benzyloxy-3,4-epoxycyclopentane

: 1066-54-2
trimethylsilylacetylene

: 1005006-73-4
C₂₀H₂₃ClO₃

: 1005006-72-3
(1S,2R,3S,5S)-2-benzyloxy-3-benzyloxymethyl-5-(trimethylsilylethynyl)cyclopentanol

Guidance literature:: trimethylsilylacetylene; With n-butyllithium; In hexane; toluene; at -78 ℃; for 0.5h;

With diethylaluminium chloride; In hexane; toluene; at 10 ℃; for 5h;

(1S,2R,3S,4S)-1-benzyloxymethyl-2-benzyloxy-3,4-epoxycyclopentane; In hexane; toluene; at 0 - 20 ℃; for 3.75h; Further stages.;
DOI:10.1016/j.tet.2007.10.054