C₁₁H₉IO₂S₂

Base Information

Chemical Name:C₁₁H₉IO₂S₂
CAS No.:1423707-58-7
Molecular Formula:C₁₁H₉IO₂S₂
Molecular Weight:364.228
Hs Code.:

C<sub>11</sub>H<sub>9</sub>IO<sub>2</sub>S<sub>2</sub>

Synonyms:C₁₁H₉IO₂S₂

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Chemical Property of C₁₁H₉IO₂S₂

Chemical Property:

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Technology Process of C₁₁H₉IO₂S₂

There total 1 articles about C₁₁H₉IO₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-96-1
3-bromo-2-thiophenecarboxaldehyde

: 1423707-58-7
C₁₁H₉IO₂S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 70 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

3.1: triphenylphosphine / dichloromethane / 0 - 20 °C / Inert atmosphere

3.2: 16 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

4.2: 5 h / 0 - 20 °C / Inert atmosphere

5.1: lithium hydroxide / water / 16 h / Reflux

5.2: pH Ca_. 2

6.1: potassium carbonate / acetonitrile / 16 h / Reflux

7.1: N-iodo-succinimide; 2,6-dimethylpyridine / 20 °C

With 2,6-dimethylpyridine; N-iodo-succinimide; lithium aluminium tetrahydride; sodium hydride; potassium carbonate; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield: 88.0%

: 1423707-58-7
C₁₁H₉IO₂S₂

: 1620074-63-6
C₁₅H₁₅N₃O₂

: 1620074-61-4
C₂₆H₂₃N₃O₄S₂

Guidance literature:: C₁₁H₉IO₂S₂; With copper(l) iodide; triethylamine; phenylacetylene; In N,N-dimethyl-formamide; for 0.0333333h;

C₁₅H₁₅N₃O₂; In N,N-dimethyl-formamide; for 2h;

Reference yield:

: 1423707-58-7
C₁₁H₉IO₂S₂

: 1620074-61-4
C₂₆H₂₃N₃O₄S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1,2-dimethoxyethane / 2 h

2.1: tetrabutyl ammonium fluoride / dichloromethane / 2 h

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

3.2: -78 °C

4.1: palladium diacetate; triphenylphosphine / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; palladium diacetate; triethylamine; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane;