Technology Process of 4-((dibenzylamino)methyl)benzonitrile
There total 8 articles about 4-((dibenzylamino)methyl)benzonitrile which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,1,3,3-Tetramethyldisiloxane; [((CH3)5C5)IrCl((CH3)2NC6H3C5H4N)]; trityl tetrakis(pentafluorophenyl)borate;
In
1,1,2,2-tetrachloroethane;
at 100 ℃;
for 20h;
chemoselective reaction;
Inert atmosphere;
Schlenk technique;
Glovebox;
DOI:10.1002/cctc.201700400
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 20 °C
2: bis(trimethylsilyl)amide yttrium(III) / toluene / 24 h / 100 °C / Inert atmosphere; Schlenk technique; Sealed tube
3: sodium hydroxide / water / Inert atmosphere
4: triethylamine / dichloromethane / 20 °C
5: bis(trimethylsilyl)amide yttrium(III); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane / toluene / 24 h / 100 °C / Sealed tube; Inert atmosphere; Schlenk technique
With
bis(trimethylsilyl)amide yttrium(III); triethylamine; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; sodium hydroxide;
In
dichloromethane; water; toluene;
DOI:10.1021/acs.orglett.9b04606
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bis(trimethylsilyl)amide yttrium(III) / toluene / 24 h / 100 °C / Inert atmosphere; Schlenk technique; Sealed tube
2: sodium hydroxide / water / Inert atmosphere
3: triethylamine / dichloromethane / 20 °C
4: bis(trimethylsilyl)amide yttrium(III); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane / toluene / 24 h / 100 °C / Sealed tube; Inert atmosphere; Schlenk technique
With
bis(trimethylsilyl)amide yttrium(III); triethylamine; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; sodium hydroxide;
In
dichloromethane; water; toluene;
DOI:10.1021/acs.orglett.9b04606
