C₂₈H₃₈O₄SSi

Base Information

Chemical Name:C₂₈H₃₈O₄SSi
CAS No.:1268455-43-1
Molecular Formula:C₂₈H₃₈O₄SSi
Molecular Weight:498.759
Hs Code.:

C<sub>28</sub>H<sub>38</sub>O<sub>4</sub>SSi

Synonyms:C₂₈H₃₈O₄SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₈O₄SSi

Chemical Property:

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Technology Process of C₂₈H₃₈O₄SSi

There total 12 articles about C₂₈H₃₈O₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268455-62-4
C₂₁H₃₂O₅Si

: 106-45-6
para-thiocresol

: 1268455-43-1
C₂₈H₃₈O₄SSi

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol1031409

Reference yield:

: 1268455-52-2
C₂₄H₃₈O₄Si

: 1268455-43-1
C₂₈H₃₈O₄SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: methanol; camphor-10-sulfonic acid / dichloromethane / 12 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 14.5 h / 50 °C

5.1: methanol; camphor-10-sulfonic acid / dichloromethane / 2 h / 0 °C

6.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 0.5 h / 0 °C

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 20 °C

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

With 1H-imidazole; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; sodium hydride; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;
DOI:10.1021/ol1031409

Reference yield:

: C₂₁H₃₂O₄Si

: 1268455-43-1
C₂₈H₃₈O₄SSi

Guidance literature:: Multi-step reaction with 2 steps

1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 20 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; dicyclohexyl-carbodiimide; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol1031409