3x ¹³C enterolactone

Base Information

• Chemical Name: 3x ¹³C enterolactone
• CAS No.: 741283-63-6
• Molecular Formula: C₁₈H₁₈O₄
• Molecular Weight: 301.306

Synonyms:3x ¹³C enterolactone

Chemical Property of 3x ¹³C enterolactone

Chemical Property:

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Technology Process of 3x ¹³C enterolactone

There total 1 articles about 3x ¹³C enterolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

3,4-bis-(3'-methoxy-[13C]-benzyl)dihydro-2(3H)-furanone (741283-62-5) → 3x 13C enterolactone (741283-63-6,918502-72-4)

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; for 2.5h;

Reference yield: 39.0%

3x 13C enterolactone (741283-63-6,918502-72-4) → 3x 13C enterodiol (741283-64-7,918502-74-6)

Guidance literature:

3x ¹³C enterolactone; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃;

With sulfuric acid; In tetrahydrofuran; water; at 0 ℃;

upstream raw materials:

3,4-bis-(3'-methoxy-[¹³C]-benzyl)dihydro-2(3H)-furanone

Downstream raw materials:

3x ¹³C enterodiol

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